| Solvent | 1H Chem. Shift |
number of lines in the multiplet | JHD (Hz) |
chem.Shift of HOD in that solvent | C13 Chem. Shift |
number of lines in the multiplet | J CD (Hz) |
Boiling point | Melting Point |
|---|---|---|---|---|---|---|---|---|---|
|
Acetic Acid-d4
|
11.65
2.04 |
1
5 |
--
2.2 |
11.5
|
178.99
20.0 |
1
7 |
--
20 |
118
|
17
|
|
Acetone-d6
|
2.05
|
5
|
2.2
|
2.8
|
206.68
29.92 |
13
7 |
0.9
19.4 |
57
|
-94
|
|
Acetonitrile-d3
|
1.94
|
5
|
2.5
|
2.1
|
118.69
1.39 |
1
7 |
--
21 |
82
|
-45
|
|
Benzene-d6
|
7.16
|
1
|
--
|
0.4
|
128.39
|
3
|
24.3
|
80
|
5
|
|
Chloroform-d
|
7.27
|
1
|
--
|
1.5
|
77.23
|
3
|
32.0
|
62
|
-64
|
|
Cyclohexane-d12
|
1.38
|
1
|
--
|
--
|
26.43
|
5
|
19
|
81
|
6
|
|
Deuterium Oxide
|
4.80 (DSS)
|
1
|
--
|
4.8
|
--
|
--
|
--
|
101.4
|
3.8
|
|
N,N-Dimethyl-formamide
|
8.03
2.92 2.75 |
1
5 5 |
--
1.9 1.9 |
3.5
|
163.15
34.89 29.76 |
3
7 7 |
29.4
21.0 21.1 |
153
|
-61
|
|
Dimethyl Sulfoxide-d6
|
2.50
|
5
|
1.9
|
3.3
|
39.51
|
7
|
21.0
|
189
|
18
|
| p-Dioxane-d6 | 3.53 | m | -- | 2.4 | 66.66 | 5 | 21.9 | 101 | 12 |
| Ethanol-d6 | 5.29 3.56 1.11 |
1 1 m |
-- | 5.3 | -- 56.96 17.31 |
-- 5 7 |
-- 22 19 |
79 | <-130 |
| Methanol-d4 | 4.87 3.31 |
1 5 |
-- 1.7 |
4.9 | -- 49.15 |
-- 5 |
-- 21.4 |
65 | -98 |
| Methylene Chloride-d2 | 5.32 | 3 | 1.1 | 1.5 | 54.00 | 5 | 24.2 | 40 | -95 |
| Pyridine-d5 | 8.74 7.58 7.22 |
1 1 1 |
-- | 5.0 | 150.35 135.91 123.87 |
3 3 5 |
27.5 24.5 25 |
116 | -42 |
| Tetrahydrofuran-d8 | 3.58 1.73 |
1 1 |
-- | 2.4-2.5 | 67.57 25.37 |
5 5 |
22.2 20.2 |
66 | -109 |
| Toluene-d8 | -- 7.09 7.00 6.98 2.09 |
-- m 1 m 5 |
-- -- -- -- 2.3 |
0.4 |
137.86 129.24 128.33 125.49 20.4 |
1 3 3 3 7 |
-- 23 24 24 19 |
111 | -95 |
| Trifluoroacetic Acid-d | 11.50 | 1 | -- | 11.5 | 164.2 116.6 |
4 4 |
72 | -15 | |
|
Trifluoroethanol-d3
|
5.02
3.88 |
1
4x3 |
--
2 (9) |
5
|
126.3
61.5 |
4
4x5 |
--
22 |
75
|
-44
|
From CIL NMR solvent Data Chart