Chemical shifts of selected compounds in Different solvents
Compounds
CDCl3
Acetone-d6
DMSO-d6
Benzene-D6
CD3CN
CD3OD
D2O
Solvent residual peak
7.26
2.05
2.50
7.16
1.94
3.31
4.79
H2O
1.56
2.84
3.33
0.40
2.13
4.87
Acetic acid
2.10
1.96
1.91
1.55
1.96
1.99
2.08
acetone
2.17
2.09
2.09
1.55
2.08
2.15
2.22
Acetonitrile
2.10
2.05
2.07
1.55
1.96
2.03
2.06
Benzene
7.36
7.36
7.37
7.15
7.37
7.33
tert-Butul alcohol
1.28
1.18
1.11
1.05
1.16
1.40
1.24
 
4.19
1.55
2.18
tert-Butul methyl ether
1.19
1.13
1.11
1.07
1.14
1.15
1.21
 
3.22
3.13
3.08
3.04
3.13
3.20
3.22
BHT
6.98
6.96
6.87
7.05
6.97
6.92
2, 6-Dimethyl-4-tert-butylphenol
5.01
6.65
4.79
5.20
 
2.27
2.22
2.18
2.24
2.22
2.21
 
1.43
1.41
1.36
1.38
1.39
1.40
Chloroform
7.26
8.02
8.32
6.15
7.58
7.90
Cyclohexane
1.43
1.43
1.40
1.40
1.44
1.45
1,2-Dichloroethane
3.73
3.87
3.90
2.90
3.81
3.78
Dichloromethane
5.30
5.63
5.76
4.27
5.44
5.49
Diethyl ether
1.21
1.11
1.09
1.11
1.12
1.18
1.17
 
3.48
3.41
3.38
3.26
3.42
3.49
3.56
Diglyme
3.65
3.56
3.51
3.46
3.53
3.61
3.67
 
3.57
3.47
3.38
3.34
3.45
3.58
3.61
 
3.39
3.28
3.24
3.11
3.29
3.35
3.37
1, 2-Dimethoxyethane
3.40
3.28
3.24
3.12
3.28
3.35
3.37
 
3.55
3.46
3.43
3.33
3.45
3.52
3.60
Dimethyl acetamide
2.09
1.97
1.96
1.60
1.97
2.07
2.08
 
3.02
3.00
2.94
2.57
2.96
3.31
3.06
 
2.94
2.83
2.78
2.05
2.83
2.92
2.90
Dimethylformamide
8.02
7.96
7.95
7.63
7.92
7.97
7.92
 
2.96
2.94
2.89
2.89
2.89
2.99
3.01
 
2.88
2.78
2.93
2.73
2.77
2.86
2.85
Dimethyl sulfoxide
2.62
2.52
2.54
1.68
2.50
2.65
2.71
Dioxane
3.71
3.59
3.57
3.35
3.60
3.66
3.75
Ethanol
1.25
1.12
1.06
0.96
1.12
1.19
1.17
 
3.72
3.57
3.44
3.34
3.54
3.60
3.65
 
1.32
3.39
4.63
2.47
Ethyl acetate
2.05
1.97
1.99
1.65
1.97
2.01
2.07
 
4.12
4.05
4.03
3.89
4.06
4.09
4.14
 
1.26
1.20
1.17
0.92
1.20
1.24
1.24
Ethyl methyl ketone
2.14
2.07
2.07
1.58
2.06
2.12
2.19
 
2.46
2.45
2.43
1.81
2.43
2.50
3.18
 
1.06
0.96
0.91
0.85
0.10
1.01
1.26
Ethylene glycol
3.76
3.28
3.34
3.41
3.51
3.59
3.65
"grease"
0.86
0.87
0.92
0.86
0.88
 
1.26
1.29
1.36
1.27
1.29
n-Hexane
0.88
0.88
0.86
0.89
0.89
0.90
 
1.26
1.28
1.25
1.24
1.28
1.29
HMPA
2.65
2.59
2.53
2.40
2.57
2.64
2.61
hexamethyphosphoramide
Methanol
3.49
3.31
3.16
3.07
3.28
3.34
3.34
 
1.09
3.12
4.01
2.16
Nitromethane
4.33
4.43
4.42
2.94
4.31
4.34
4.40
n-Pentane
0.88
0.88
0.86
0.87
0.89
0.90
 
1.27
1.27
1.27
1.23
1.29
1.29
2-Propanol
1.22
1.10
1.04
0.95
1.09
1.50
1.17
 
4.04
3.90
3.78
3.67
3.87
3.92
4.02
Pyridine
8.62
8.58
8.58
8.53
8.57
8.53
8.52
 
7.29
7.35
7.39
6.66
7.33
7.44
7.45
 
7.68
7.76
7.79
6.98
7.73
7.85
7.87
Silicone grease
0.07
0.13
0.29
0.08
0.10
Poly(dimethylsiloxane)
Tetrahydrofurane
1.85
1.79
1.76
1.40
1.80
1.87
1.88
 
3.76
3.63
3.60
3.57
3.64
3.71
3.74
Toluene
2.36
2.32
2.30
2.11
2.33
2.32
 
7.17
7.1-7.2
7.18
7.02
7.1-7.3
7.16
 
7.25
7.1-7.2
7.25
7.13
7.1-7.3
7.16
Triethyl amine
1.03
0.96
0.93
0.96
0.96
1.05
0.99
 
2.52
2.45
2.43
2.40
2.45
2.58
2.57
From CIL Catalog
H.Gottlieb, V.Kotlyar, A.Nudelman, NMR Chemical Shifts of Common Laboratory Solvents as Trace Impurities, J.Org.Chem., 62, 1997.